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In this work, aiming at the identification of the aglycones divicine and isouramil in doughs through LC-ESI-MS, a procedure to distinguish the forms generated from the spontaneous fragmentation of vicine and convicine inside the ESI source and/or the ion optics of the LCQ spectrometer from those deriving from the degradation of the compounds during the dough incubation, was developed and confirmed by the analysis of the enzymatic hydrolysis of the vicine/convicine extracts
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[DOI] [PubMed] [Google Scholar] 42.Nutraceuticals in acute and prophylactic treatment of migraine
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