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Supplementary material The Supplementary Material for this article can be found online at: References 1 MoureUAETanTShaLLuXShaoZYangGet al

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The column was eluted at a flow rate of 400 L/min with initial conditions of 10% mobile phase A (20 mM ammonium acetate and 20 mM ammonium hydroxide in water) and 90% mobile phase B (10 mM ammonium hydroxide in 75:25 v/v acetonitrile/methanol) followed by a 10 min linear gradient to 100% mobile phase A

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doi:10.1007/s00726-017-2493-3 Khanna P, Aeri BT