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Samples were reconstituted in 100 L and 2 L of the sample was injected from a 4 C autosampler into a ZIC-pHILIC 150 2.1 mm 5 m particle size column (EMD Millipore) with a ZIC-pHILIC 20 x 2.1 guard column in a Vanquish Duo UHPLC System (Thermo Fisher Scientific) at 25 C

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One of the three key diagnostic criteria for AP is a serum lipase or amylase concentration exceeding the normal range by threefold or more [116]

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