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reaction solution was analyzed using reverse-phase HPLC with Luna 3 C18 column (4.6 50 mm) using solvent A (0.1% TFA in water) and solvent B (0.1% TFA in Acetonitrile) with a gradient of 10% to 70% of solvent B in 10 minutes at 50 C

[DOI] [PubMed] [Google Scholar] Fosgerau K

That means that virtually any protein, carbohydrate, lipid or nucleic acid is a potential target for the toxic action of the highly toxic HO radical with its extremely high reactivity (Lenzen 2017

In: Burk, R.F., Ed

Both are antioxidants that can work synergistically to enhance each other's effects

Inspect the peptide vial: confirm the powder is dry, intact, and not clumped or moist