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Synthesis of 2,2-dithiobis(ethanesulfonate) (diMESNA) MESNA (3.28 g, 0.02 mol) was dissolved in water (100 mL) and added to a solution of 2,2 dithiobis(benzothiozole) (3.32 g, 0.01 mol) in chloroform (250 mL)

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